Volume 11, Issue 2: 36-45; March 25, 2021  
NUTRITIONAL COMPOSITION, IN VITRO GAS PRODUCTION AND IN  
SACCO DEGRADABILITY OF PROCESSED Croton megalocarpus NUTS  
FOR RUMINANT FEEDING  
Elias KABOCHI NJOROGE, Caroline CELINA WAMBUI and Chrilukovian BWIRE WASIKE  
Livestock Efficiency Enhancement Group (LEEG), Department of Animal Science, School of Agriculture & Food Security, Maseno  
University, P.O. Private Bag, 40105, Maseno, Kenya  
Email: wambuicc@gmail.com;  
Supporting Information  
ABSTRACT: This study was conducted to evaluate the effects of processed croton nut on chemical  
composition, in vitro gas production and in sacco degradability. Four forms of croton nut namely: whole nut  
(WN), peeled nut (PN), De-husked nut (DhN) and De-fatted seed (DfS) were subjected to proximate analysis,  
Van Soest fibre fractionation, mineral composition analysis, phytochemical and aflatoxin tests. Degradability  
analyses were conducted using in vitro gas production and in sacco degradability techniques. Defatted seeds  
recorded significantly high level of CP and NFE (198 g/kg and 174 g/kg), whereas, ash content and ether  
extract (EE) were significantly high in WN (59 g/kg) and DhN (362 g/kg) respectively. Low fibre fractions of  
NDF (556 g/kg) and ADF (490 g/kg) were observed in DhN, while the mineral content was high in DfS which  
had calcium at 2.13 g/kg and phosphorus at 5.04 g/kg. High level of flavonoid was recorded in WN (124  
g/kg), whereas low level of alkaloids was found in DfS (60 g/kg) and tannins in PN (7.1 g/kg). The potential  
in vitro gas production (a+b) was highest in DfS (22.2 ml/0.2 gDM) while potential in sacco degradability  
(a+b) was highest in DhN (58.4 %). High level of organic matter digestibility (OMD) (41 %) was observed in  
DfS. At kp=0.025 rumen outflow rate, DhN had the highest effective degradability of dry matter (56.6%),  
while the rate effective crude protein degradability was 80.0 %. Processing through peeling and dehusking  
improved the protein, energy and mineral content of DhN and DfS while crude fibre content reduced.  
Nutritional composition and degradability characteristics of all forms of croton nuts imply that they could be  
used in a total mixed ration (TMR) to supply requisite nutrients for maintenance of ruminant animals, while  
DhN and DfS could be used to supplement energy and protein for increased productivity.  
Keywords: Chemical composition, Croton nut, degradability, Gas production technique, Processing.  
Abbreviations: WN: whole nut; PN: peeled nut; DhN: dehusked nut; DfS: defatted seeds  
INTRODUCTION  
The livestock sector accounts for 40% of agriculture’s Gross Domestic Product (GDP) in developing countries and is not  
only a source of food and livelihood but enhances resilience against climate change extremities such as drought (Herrero  
et al., 2013; Nabarro and Wannous, 2014). The continuously growing human population as well as increased per capita  
income has led to increased demand for livestock-based products (Otte et al., 2019). Thus, livestock production ought to  
increase so as to meet the rising demand. Ruminant animals in tropical arid and semi-arid areas (ASAL) continue to play  
a key role of the rural households in developing countries where they are a major source of nourishment from products  
such as meat and milk as well as play social economic roles by providing income and acting as an economic safety net  
Livestock production in the tropics is constrained by various factors which include inadequate nutrition, breeding and  
reproduction, disease and parasites among others (Kahi and Wasike, 2019). In confined systems, feeds account for up to  
70% of the total cost of production (Makkar, 2014). Hence, variation in quantity and quality of feeds becomes a major  
constraint to livestock production. The problem of feed scarcity is further exacerbated by increased food feed  
competition between human and livestock and decline in available land for feed production. Majority of ruminant animals  
(cattle, sheep and goats) in Kenya are reared in arid and semi-arid Counties (KNBS, 2019). In these areas, effects of  
climate change such as drought greatly reduces available feed resources consequently leading to low productivity and at  
time causing mortality of the animals (Makkar, 2014). Feeding strategies that optimise utilisation of available feed  
resources are thus critical to maintain ruminant productivity and preventing mortality.  
Identification and introduction of alternative feed resources is a major avenue that could be used to mitigate feed  
scarcity. Locally available, low-cost feed resources could enhance resilience and adaptability of small holder farmers and  
pastoralists by allowing them to transit through adverse effects of climate change (Makkar, 2014). Evaluation of non-  
conventional feed resources for potential inclusion in mainstream livestock offers a preliminary step in determining the  
suitability of the identified feed resource before it can be included in livestock diets (Quansah and Makkar, 2012). One  
36  
Citation: Kabochi Njoroge E, Celina Wambui C and Bwire Wasike C (2021). Nutritional composition, in vitro gas production and in sacco degradability of processed  
Croton megalocarpus nuts for ruminant feeding. Online J. Anim. Feed Res., 11(2): 36-45. DOI: https://dx.doi.org/10.51227/ojafr.2021.7  
such feed with potential is croton nuts from Croton megalocarpus tree. Croton tree is adapted to different agro-ecological  
zones in the tropics and has multipurpose use such as provision of wood fuel, acting as a live fence and a source of bio  
fuel (Ndegwa et al., 2011). Croton tree produces up to 25 kg of nuts per year (Jacobson et al., 2018) which are reported to  
contain high CP content of up to 18%, crude fat (30%) and hence could be exploited for feeding livestock (Thijssen et al.,  
1996; Ndegwa et al., 2011). Farmers have been observed to collect and use croton nuts for feeding cows and goats  
during extreme dry seasons. However, there is limited information on the chemical composition, ant - nutritive factors and  
degradability of croton nuts. Moreover, there is also limited information on effects of processing various forms of croton  
such as peeling, dehusking and oil extraction on the nutritive value for effective utilization of this underutilized feed  
resource. This study was therefore conducted to evaluate nutritional and phytochemical composition and ruminal  
degradation of the various processed forms of croton nut to facilitate its use in ruminant feeding.  
MATERIALS AND METHODS  
Site description  
Samples of Croton nut were collected from Laikipia West and East sub counties of Laikipia County, which is located  
North - West of Mount Kenya at an altitude of between 1600 m and 2300 m above sea level with a total area of 9,700  
km2. The area experiences a bimodal rainfall pattern with long rains between March and June and short rains between  
October and December separated by dry seasons (MoALF, 2017). The annual precipitation varies between 400 mm to  
900 mm and average temperature is between 16 oC and 26 oC. The area lies in semi - humid, semi - arid, arid to very arid  
agro ecological zones IV - VII, and is considered arid and semi-arid (ASAL) (MoALF, 2017).  
Collection and processing of croton nuts  
Mature croton nuts were collected from the ground, air dried under shade and processed into four forms which  
included whole nuts (WN), peeled nut (PN), dehusked nut (DhN) and defatted seeds (DfS). The whole nuts (WN) form  
comprised of unprocessed whole croton nuts with the outer peel (exocarp) and the hard woody husk (endocarp) intact.  
Peeled nuts (PN) consisted of nuts whose outer seed coat (peel/exocarp) was removed leaving the hard woody endocarp  
intact. De-husked nuts (DhN) consisted of the inner seeds after the removal of both the outer peel (exocarp) and the hard  
woody husk (endocarp). Defatted seeds (DfS) also referred to as Croton cake was the by-product of the seeds after oil  
extraction using a cold press. The DfS form was obtained from a commercial plant that extracts bio-diesel from croton in  
Laikipia County. After processing into various forms, the samples were then ground using a hummer mill to pass through  
a 2 mm screen and stored in air tight glass containers pending analyses.  
Chemical analyses  
Ground samples of the various processed forms of croton were subjected to proximate analysis to determine dry  
matter (DM), ash, crude fibre (CF), ether extract (EE) and crude protein (CP) which were expressed on dry matter basis  
according to AOAC (1990). Nitrogen free extract (NFE) was calculated as the difference of the sum (%) of crude protein,  
crude fibre, ether extract and total ash from 100%. Neutral detergent fibre (NDF), acid detergent fibre (ADF) and acid  
detergent lignin (ADL), were sequentially determined using the method of Van Soest et al. (1991). Hemicellulose content  
was calculated as the difference between NDF and ADF, whereas cellulose was the difference between ADF and ADL.  
Gross energy (MJ/kg) was determined from 0.5 g of sample using a digital bomb calorimeter (CAL2K of Digital Data  
Systems (pty) ltd South Africa). Neutral detergent insoluble nitrogen and acid detergent insoluble nitrogen were  
determined from the residues of NDF and ADF using Kjeldahl method (AOAC, 1990). Nitrogen obtained was multiplied  
with a conversion factor (6.25) to obtain neutral detergent insoluble crude protein (NDICP) and acid detergent insoluble  
crude protein (ADICP).  
Sodium (Na) and potassium (K) concentration was determined using atomic emission in a flame photometer while  
total available phosphorus (P) concentration was determined using Ultra Violet (UV) colorimeter (AOAC, 1990). Calcium  
(Ca), magnesium (Mg), iron (Fe), zinc (Zn), manganese (Mn) and copper (Cu) concentrations were determined using an  
atomic absorption spectrophotometer (AAS) (AOAC, 1990).  
Phytochemicals and aflatoxin analyses  
Flavonoids were extracted from the samples using organic solvents and expressed gravimetrically as outlined by  
Harbone (1984). Alkaloid determination was done by extraction from the samples using acetic acid dissolved in ethanol  
(Harbone, 1984). Tannin content was determined using Folin-Coicalteu reagent and determination of absorbance was  
done at 725 nm using a UV-visible spectrophotometer (AOAC, 1990). Aflatoxins were extracted using methanol and levels  
determined by ELISA testing kit. The amount of aflatoxin was expressed in parts per billion (ppb) calculated from the  
standard aflatoxin curve (Leszczyñska et al., 2001).  
In vitro gas production  
In vitro gas procedure was conducted following the procedure of Menke and Steingass (1988). Rumen liquor was  
drawn in the morning from two mature fistulated Friesian steers. The steers had 450±25 kg live weight and were fed on  
Rhodes grass (Chloris gayana) hay and wheat bran at 90% and 10% respectively of the total ration at 3% of their body  
37  
Citation: Kabochi Njoroge E, Celina Wambui C and Bwire Wasike C (2021). Nutritional composition, in vitro gas production and in sacco degradability of processed  
Croton megalocarpus nuts for ruminant feeding. Online J. Anim. Feed Res., 11(2): 36-45. DOI: https://dx.doi.org/10.51227/ojafr.2021.7  
weight at 08:00 hours and 17:00 hours for maintenance purposes. Mineral licks and water were provided adlibitum. This  
was done so as to maintain a stable rumen environment before the rumen liqour was collected. Collected rumen liqour  
was strained through four layers of cheese cloth into a pre-warmed, vacuum flask and kept at 39oC under CO2  
atmosphere. About 0.2g of 1mm ground samples (WN, PN, DhN and DfS) were weighed into the glass syringes. A mixture  
of 30ml of rumen liquor and buffer in the ratio of 1:2 was added into each of the 100ml calibrated glass syringes that  
were pre-warmed to 39oC. Oil was applied to the pistons to facilitate ease of movement and prevent gas escape. Two  
blank syringes with rumen liquor without a feed sample were included as controls. All syringes were incubated in a water  
bath maintained at 39oC and shook periodically. Gas production readings were recorded at 0 and after 3, 9, 12, 24, 48,  
72 and 96 hours of incubation.  
The gas production characteristics were computed by fitting the mean gas volumes to the exponential equation of  
Ørskov and Mcdonald (1979) using Neway Excel Computer program (Chen X. B., Rowett Research Institute, Aberdeen UK).  
     ꢃꢄꢅ ꢇꢈꢉꢊꢋ  
(1)  
Where: Y is gas production (ml/0.2g) at time t, a is gas production (ml) from immediately soluble fraction, b is gas  
production (ml) from insoluble fraction, a+b is gas production from potential degradable fraction, c is the rate constant of  
gas production per hour (h), t is the incubation time in hours and e is the exponential constant (2.718).  
In vitro gas production parameters were used to estimate organic matter digestibility (OMD), metabolisable energy  
(ME), Dry Matter intake (DMI) and short chain fatty acids (SCFA) using the models presented in Equations 2 to 5.  
ꢍꢎꢏ   ꢅꢑꢒꢓꢓ  ꢔꢒꢓꢓꢕꢇꢖꢗ  ꢔꢒꢑꢘꢇꢙꢚ  ꢔꢒꢔꢛꢘꢅꢇꢜꢝ  
(2)  
(3)  
(4)  
(5)  
ꢎꢞ(MJ/Kg) ꢟꢒꢟꢔ  ꢔꢒꢅꢠꢛꢇꢖꢗ  ꢔꢒꢔꢘꢡꢇꢙꢚ  
ꢏꢎꢢ(kg/day) ꢅꢒꢛꢛ  ꢔꢒꢑꢕꢁ  ꢔꢒꢔꢟꢕꢡꢃ  ꢑꢣ  
ꢤꢙꢥꢝ ꢦꢦꢧꢨꢩꢪ  ꢔꢒꢔꢟꢟꢟꢇꢖꢗ  ꢔꢒꢔꢔꢑꢟꢘ  
Where: GV is gas production after 24 hours, CP is crude protein and XA ash content of the processed form of croton,  
a, b and c are constants as described in Equation 1.  
In sacco degradation (nylon bag technique)  
In sacco degradation of the various forms of croton was carried out using Nylon bag technique as described by  
Ørskov (2000). Two mature fistulated Friesian steers weighing 450±25 kg live weight were used. The steers were fed on  
Rhodes grass (Chloris gayana) hay and wheat bran at 90% and 10% respectively of the total ration at 3% of their body  
weight at 08:00 hours and 17:00 hours for maintanance purposes. Mineral licks and water were provided adlibitum. This  
was done so as to maintain a stable rumen environment. Five grams of each processed sample of croton was weighed  
into duplicate nylon bags (12cm by 6cm, 50µm pore size). The bags were incubated for 0, 9, 12, 16, 24, 48 and 72 hours  
in the rumen. Zero-hour washing was measured by soaking nylon bags containing the sample in water maintained at 39  
oC for 1 hour. Bags from zero hour washing and those retrieved from the rumen were washed thoroughly under running  
cold water for 15 minutes until the washing water was clear. The bags with the residue were then dried at 60oC for 48  
hours in a forced air oven and dry matter loss determined as the difference from the original weight. Crude protein and  
neutral detergent fibre (NDF) from the residue were then analysed. The DM, CP and NDF degradability characteristics were  
determined by fitting the degradability data to the exponential Equation 6 of Ørskov and Mcdonald (1979) using Neway  
Excel Computer program (Chen X. B., Rowett Research Institute, Aberdeen UK).  
    ꢃꢄꢅ ꢇꢈꢉꢊꢋ  
(6)  
Where: P is the degradability of (DM, CP and NDF) incubated in the rumen at time t in hours, a is the percentage of  
rapidly soluble fraction, b is the percentage of insoluble but fermentable fraction, a+b is potential percentage of  
degradability, c is the rate of constant degradation per hour (h-1) and e is the exponential constant (2.718).  
Effective degradability (ED) of DM, CP and NDF was calculated using Equation (7).  
ꢞꢏ    ꢃꢄꢊꢫꢬꢭ  
(McDonald, 1981)  
(7)  
Where: a+b is the potential degradability, c is the rate constant degradability per hour (h), kp is the ruminal outflow  
rate. The following outflow rates (kp) per hour were considered (0.025, 0.05 and 0.08). Rumen undegradable protein  
(RUP) was calculated by subtracting effective degradable CP% from 100%. The DM index value (IV) which denotes the  
fraction of the feed that would provide nutrients to the animal for its maintenance needs was calculated using Equation 8.  
A feed with an index value above 33 would provide sufficient nutrients to the animal for its maintenance needs.  
ꢢꢗ    ꢔꢒꢑꢃ  ꢟꢔꢔꢣ  
Where: a, b and c are as described in Equation 6.  
Statistical analysis  
Analysis of variance (ANOVA) was carried out on proximate composition, fibre fractions, minerals composition, gross  
energy (GE) and phytochemicals as well as in vitro gas production and in sacco degradability parameters. The analysis  
was based on completely randomized design using STATA (2017). Significant differences between the means were tested  
using Tukey’s honest significance difference (THSD). The following statistical model was used  
ꢯꢰ      ꢯꢰ  
(9)  
38  
Citation: Kabochi Njoroge E, Celina Wambui C and Bwire Wasike C (2021). Nutritional composition, in vitro gas production and in sacco degradability of processed  
Croton megalocarpus nuts for ruminant feeding. Online J. Anim. Feed Res., 11(2): 36-45. DOI: https://dx.doi.org/10.51227/ojafr.2021.7  
Where: yij = chemical composition, in vitro gas production and in sacco degradability parameters,  = mean of the  
different forms of Croton megalocarpus, fi = forms of croton nuts (i= WN, PN, DhN and DfS), eij = error term.  
Ethical approval  
All process of in vivo study was in according to animal welfare rules and approved by university ethical committee.  
RESULTS  
Proximate composition  
Proximate composition of the various forms of croton nut is presented in Table 1. Peeled nut had significantly high  
DM content while WN did not differ significantly from DhN and DfS (P<0.05). Defatted seeds had significantly high CP  
content compared to other forms while the lowest level of CP was recorded in WN and PN which were not significantly  
different (P<0.05). The CF content was significantly low in DhN compared to the other forms while the ash content was  
significantly high in WN followed by DfS, but no significant difference was observed between PN and DhN. The EE content  
did not differ significantly between WN and PN but was significantly high in DhN at 363g/kg and significantly low in DfS  
(113g/kg; P<0.05). The NFE in all forms did not differ significantly. Gross energy was highest in the DhN (21.1MJ/kg) and  
lowest in PN (17.3MJ/Kg) although the differences were not significant.  
Fibre composition  
Fibre composition of the various forms of croton nut is presented in Table 2. Processing by dehusking and defatting  
resulted to lower NDF content in DhN and DfS to 576 g/kg and 556g/kg respectively, compared to WN and PN forms  
(P<0.05). Hemicellulose content was highest in PN (205 g/kg) (P<0.05). The cellulose level ranged between 94g/kg in  
DhN to 181g/kg in WN. The NDICP ranged between 16 in PN to 24 in DfS while ADICP ranged between 16 to 21 in both  
WN and DfS (P>0.05). There were no significant differences in ADF, ADL, cellulose, NDICP and ADICP among the croton  
forms (P>0.05).  
Table 1 - Proximate composition of the various forms of croton nut (g/kg)  
Nutritional  
parameter  
Whole nut  
(WN)  
Peeled nut  
(PN)  
Dehusked nut  
(DhN)  
Defatted seeds  
(DfS)  
SEM  
Prob.  
Dry matter  
893a  
89a  
522a  
185a  
59a  
963b  
80a  
579b  
175a  
23b  
917c  
158b  
336c  
363b  
24b  
919c  
198c  
476a  
113c  
38c  
0.763  
1.487  
2.747  
2.824  
0.449  
0.847  
0.826  
P<0.001  
P<0.001  
P<0.001  
P<0.001  
P<0.001  
P<0.001  
NS  
Crude protein  
Crude fibre  
Ether extract  
Ash  
Nitrogen free extract  
143a  
143 a  
120 a  
174 a  
Gross energy (MJ/kg)  
18.1  
17.3  
21.1  
19.3  
a,b,c;  
Means in the same row without common letter are different at P<0.05; SEM = standard error of the mean; Prob.= probability; NS = not  
significant.  
Table 2 - Fibre composition of the various forms of croton nut (g/kg)  
Dehusked nut  
Defatted seeds  
Fibre components Whole nut (WN) Peeled nut (PN)  
SEM  
Prob.  
(DhN)  
576b  
482  
392  
94ac  
94  
(DfS)  
556b  
490  
367  
66c  
NDF  
686a  
506  
341  
180ab  
181  
22  
741a  
536  
377  
205b  
168  
16  
2.36  
1.10  
P<0.001  
0.357  
ADF  
ADL  
1.62  
0.781  
Hemicellulose  
Cellulose  
NDICP  
ADICP  
2.02  
P<0.010  
0.089  
132  
24  
1.39  
23  
0.159  
0.155  
21  
16  
17  
21  
0.115  
0.063  
a,b,c; Means in the same row without common letter are different at P<0.05; NDF = neutral detergent fibre; ADF = acid detergent fibre; ADL =  
acid detergent lignin; NDICP = neutral detergent insoluble crude protein; ADICP = acid detergent insoluble crude protein; SEM = standard  
error of the mean; Prob. = probability.  
Minerals composition  
Mineral content of the various forms of croton nut is presented in Table 3. Processing by defatting enhanced the  
macro minerals (Ca, P, Mg and Na) in DfS (P<0.05). Whole nut recorded the highest level of potassium (14.27 g/Kg)  
39  
Citation: Kabochi Njoroge E, Celina Wambui C and Bwire Wasike C (2021). Nutritional composition, in vitro gas production and in sacco degradability of processed  
Croton megalocarpus nuts for ruminant feeding. Online J. Anim. Feed Res., 11(2): 36-45. DOI: https://dx.doi.org/10.51227/ojafr.2021.7  
(P<0.05). Amongst the micro minerals, Fe was highest in WN (0.113 g/kg), Mn in DhN (0.047g/kg) and Zn in DfS (0.049  
g/kg) at P<0.05 compared to the other forms.  
Table 3 - Mineral composition of the various forms of croton nut (g/kg)  
Whole nut  
(WN)  
Peeled nut  
(PN)  
Dehusked nut  
(DhN)  
Defatted seeds  
(DfS)  
Mineral composition  
SEM  
Prob.  
Macro minerals  
Calcium  
1.51a  
3.21ab  
0.46ab  
0.79a  
1.69ab  
2.78a  
0.35a  
0.14b  
4.36b  
1.82ab  
4.21bc  
0.57bc  
0.34c  
2.13b  
5.04c  
0.71c  
2.27d  
5.41c  
0.084  
0.284  
0.042  
0.251  
1.294  
0.0324  
<0.001  
<0.001  
<0.001  
<0.001  
Phosphorus  
Magnesium  
Sodium  
Potassium  
Micro minerals  
Iron  
14.27a  
3.66b  
0.113a  
0.024a  
0.022ab  
0.007  
0.051b  
0.029a  
0.017a  
0.015  
0.063bc  
0.047b  
0.034bc  
0.019  
0.075c  
0.046b  
0.049c  
0.008  
0.0071  
0.0031  
0.004  
<0.001  
<0.001  
0.001  
Manganese  
Zinc  
Copper  
0.0027  
0.401  
a,b,c,d; Means in the same row without common letter are different at P<0.05; SEM = standard error of the mean; Prob. = probability.  
Phytochemicals and aflatoxin content  
Phytochemical composition and aflatoxin levels of the various forms of croton nut is presented in Table 4. Flavonoid  
content in WN was significantly higher (124 g/kg) (P<0.05) from other forms. Alkaloids ranged from 60g/kg in DfS to  
69g/kg in WN (P>0.05). Both WN and DfS had the highest tannin level (9.6 g/kg) (P<0.05). Aflatoxin level was highest in  
DhN (21.1 ppb) and least in PN (6.4 ppb).  
In vitro gas production  
In vitro gas production fermentation characteristics of the various forms of croton nut are presented in Table 5.  
There was no difference in gas production from the readily soluble fraction (a) among the forms (P>0.05). However,  
highest gas production of (b) and (a+b) were observed in DfS at (18.6 ml) and (22.2 ml) respectively (P<0.05). Defatted  
seeds recorded the highest OMD (41.0%), ME (5.9 MJ/kg), and SCFA (0.419 mmol/L) while PN had the least OMD  
(29.8%), ME (4.3 MJ/kg) and SCFA (0.271 mmol/L).  
In sacco DM degradability  
In sacco DM degradability characteristics of the various forms of croton nut are presented in Table 6. Dehusked nut  
had highest rapidly soluble DM fraction (a ~ 42.8%) and potentially degradable DM fraction (a+b ~ 58.4%) (P<0.05), with  
the rate constant of degradation (c) ranging between 0.02 in WN to 0.2 in DhN. Effective dry matter degradability (EDDM)  
among the various forms was observed to reduce as the rumen outflow rate increased. Dehusked nut (DhN) had  
consistently higher percentages of EDDM and at all rumen outflow rates and a converse trend was true for PN. Dehusked  
nut also recorded the highest IV 90.1 (P<0.05).  
In sacco CP degradability  
In sacco CP degradability characteristics of the various forms of croton nut are presented in Table 7. Rapidly  
degradable fraction of protein (a) was highest in WN (4.1%) (P<0.05). At p<0.05, slowly degradable fraction (b) and  
potential degradable fraction (a+b) were highest in DhN (87.8%) and (87.9%) and lowest in WN (59.4%) and (63.5%)  
respectively. The rate constant of degradability per hour (c) was highest in PN (0.26) and lowest in DhN (0.02) whereas  
highest rumen undegradable protein was recorded in WN (36.4%) and the lowest recorded in DhN (12.0%). At kp=0.025,  
effective degradable crude protein for DhN (80.0%) and DfS (65.1%) were different (P<0.05) from that of WN and PN. The  
rumen undegradable protein (RUP) among all forms of croton nuts at 0.025 kp was low compared to RUP at 0.05kp and  
0.08kp (P<0.05).  
In sacco NDF degradability  
The NDF degradability characteristics of the various forms of croton nut are presented in Table 8. Significant  
difference in NDF degradability was observed in rapidly degradable fraction (a) which was highest in DhN (17.2%)  
compared to the other forms of croton nut (P<0.05). There was no significant difference among the various forms of  
croton nut for b, a+b, and c. At 0.025kp and 0.08kp, effective degradability NDF was significantly high in DhN compared  
to the other forms. However, at 0.05kp there was no significance difference among all forms of croton nut in EDNDF.  
40  
Citation: Kabochi Njoroge E, Celina Wambui C and Bwire Wasike C (2021). Nutritional composition, in vitro gas production and in sacco degradability of processed  
Croton megalocarpus nuts for ruminant feeding. Online J. Anim. Feed Res., 11(2): 36-45. DOI: https://dx.doi.org/10.51227/ojafr.2021.7  
Table 4 - Phytochemical and aflatoxin content of the various forms of croton nut (g/kg).  
Whole nut  
(WN)  
Peeled nut  
(PN)  
Dehusked nut  
(DhN)  
Defatted seeds  
(DfS)  
Anti-nutritive factors  
SEM  
Prob.  
Flavonoids  
Alkaloids  
124a  
57b  
43b  
64b  
1.01  
1.85  
0.04  
3.13  
P<0.0014  
0.307  
69  
67  
62  
60  
Tannins  
9.6a  
14  
7.1b  
6.4  
8.9ab  
21.1  
9.6a  
9.9  
P<0.021  
Aflatoxin (ppb)  
ND  
a,b,c; Means in the same row without common letter are different at (P<0.05); SEM = standard error of the mean; Prob. = probability; ND = not  
determined.  
Table 5 - In vitro gas production of the various forms of croton nut (ml gas/0.2g dry matter).  
Whole nut  
(WN)  
Peeled nut  
(PN)  
Dehusked nut  
(DhN)  
Defatted seeds  
(DfS)  
Gas production parameters  
SEM  
Prob.  
a
1.4  
18.6a  
20.1ab  
0.08  
34.1ab  
5.0a  
4.2  
10.6b  
14.9a  
0.06  
29.8a  
4.3a  
2.4  
14.3ab  
16.8ab  
0.10  
35.3b  
5.1a  
3.7  
18.4a  
22.2b  
0.08  
41.0c  
5.9b  
0.465  
1.28  
P<0.083  
P<0.004  
P<0.019  
P<0.096  
P<0.004  
P<0.005  
P<0.103  
P<0.035  
b
a+b  
1.13  
c
0.007  
1.54  
OMD  
ME (MJ/Kg)  
DMI (kg/day)  
SCFA (mmol/L)  
0.218  
0.226  
0.022  
2.6  
0.37a  
3.8  
0.27ab  
2.8  
0.32ab  
3.6  
0.41b  
a,b,c; Means in the same row without common letter are different at P<0.05; a = gas production (ml) from immediately soluble fraction; b = gas  
production (ml) from insoluble fraction, a+b = potential gas production (ml); c = the rate constant of gas production per hour; OMD = organic  
matter digestibility; ME = metabolisable energy; DMI = dry matter intake; SCFA = short chain fatty acids; SEM = standard error of the mean ;  
Prob. = probability.  
Table 6 - In sacco DM degradability characteristics for various forms of croton nut (%).  
DM degradability  
parameters  
a
b
a+b  
c
EDDM (kp=0.025)  
EDDM (kp=0.05)  
EDDM (kp=0.08)  
Whole nut  
(WN)  
29.5a  
18.8ab  
48.3a  
0.02  
37.8a  
34.9a  
33.2a  
41.0a  
Peeled nut  
(PN)  
Dehusked nut  
(DhN)  
Defatted  
seeds (DfS)  
33.4d  
SEM  
Prob  
26.4b  
22.5b  
49.0a  
0.01  
30.7b  
28.8b  
28.0b  
36.6a  
42.8c  
15.6ab  
58.4b  
0.20  
56.6c  
55.1c  
53.8c  
90.1b  
2.33  
1.49  
1.87  
0.032  
3.56  
3.68  
3.64  
8.44  
P<0.001  
P<0.028  
P<0.011  
P<0.051  
P<0.001  
P<0.001  
P<0.001  
P<0.017  
12.5a  
46.0a  
0.05  
41.8d  
39.7d  
38.3d  
48.5a  
IV  
a,b,c,d;  
Means in the same row without common letter are different at P<0.05; a = is the rapidly soluble fraction; b = is the insoluble but  
fermentable fraction; a+b = is the potentially degradable fraction; c = is the rate constant of degradation; IV = index value; EDDM = effective  
degradability of dry matter; kp = rumen outflow rate; SEM = standard error of the mean; Prob. = probability.  
Table 7 - In sacco CP degradability characteristics of the various forms of croton nut (%).  
Whole nut  
(WN)  
Peeled nut  
(PN)  
Dehusked nut  
(DhN)  
Defatted  
seeds (DfS)  
CP degradability  
SEM  
Prob.  
a
4.1a  
0.02b  
75.0b  
75.0b  
0.26b  
68.5a  
63.0b  
57.4b  
31.4a  
36.9b  
42.5b  
0.08b  
87.8c  
87.9c  
0.02b  
80.0b  
73.5c  
66.9c  
19.9b  
26.4c  
33.0c  
0.4b  
0.660  
3.81  
P<0.002  
P<0.001  
P<0.001  
P<0.001  
P<0.001  
P<0.001  
P<0.001  
P<0.001  
P<0.001  
P<0.001  
b
59.4a  
63.5a  
0.06a  
46.2a  
36.8a  
29.8a  
53.7a  
63.1a  
70.1a  
74.7b  
75.1b  
0.16c  
65.1b  
57.5d  
50.4d  
34.8b  
42.4d  
49.5d  
a+b  
3.26  
c
0.0312  
4.59  
EDCP (kp=0.025)  
EDCP (kp=0.05)  
EDCP (kp=0.08)  
RUP (kp=0.025)  
RUP (kp=0.05)  
5.06  
5.16  
4.59  
5.06  
RUP (kp=0.08)  
5.16  
a,b,c,d;  
Means in the same row without common letter are different at P<0.05; a = is the rapidly soluble fraction; b = is the insoluble but  
fermentable fraction; a+b = is the potentially degradable fraction; c = is the rate constant of degradation; EDCP = effective degradability of  
crude protein; kp = rumen outflow rate; RUP = rumen undegradable protein; SEM = standard error of the mean; Prob. = probability.  
41  
Citation: Kabochi Njoroge E, Celina Wambui C and Bwire Wasike C (2021). Nutritional composition, in vitro gas production and in sacco degradability of processed  
Croton megalocarpus nuts for ruminant feeding. Online J. Anim. Feed Res., 11(2): 36-45. DOI: https://dx.doi.org/10.51227/ojafr.2021.7  
Table 8 - In sacco NDF degradability characteristics of the various forms of croton nuts (%)  
Whole nut  
(WN)  
6.5a  
Peeled nut Dehusked nut  
Defatted  
seeds (DfS)  
1.6a  
NDF degradability  
SEM  
Prob.  
(PN)  
2.0a  
9.4  
(DhN)  
17.2b  
10.1  
27.3  
0.33  
22.9c  
21.2  
20.1c  
A
B
2.41  
1.28  
0.002  
0.144  
15.1  
15.8  
a+b  
21.6  
11.4  
0.01  
5.9b  
7.5  
17.4  
2.44  
0.065  
C
0.03  
15.0a  
0.35  
9.1b  
0.0052  
2.47  
0.714  
EDNDF (kp=0.025)  
EDNDF (kp=0.05)  
P<0.001  
0.053  
11.2  
10.2a  
6.8  
5.5b  
2.45  
EDNDF (kp=0.08)  
a.b,c,d;  
3.7b  
2.43  
P<0.001  
Means in the same row without common letter are different at P<0.05; a = is the rapidly soluble fraction; b = is the insoluble but  
fermentable fraction; a+b = is the potentially degradable fraction; c = is the rate constant of degradation; EDNDF = effective degradability of  
neutral detergent fibre; kp = rumen outflow rate; SEM = standard error of the mean; Prob. = probability.  
DISCUSSION  
Nutritional composition  
The DM content in all forms was above 86%, which is the recommended level for storage of feeds. Conversely, this  
implied low moisture content that is critical in preventing growth of fungi and reducing aflatoxin contamination (Mahato et  
al., 2019). The high moisture content in WN suggests that the peel acts as a barrier against loss and itself contains  
moisture. Whole nuts and DfS had high ash contents indicating that they could be good sources of minerals for grazing  
animals during the dry seasons hence averting the effects of mineral deficiencies such as impaired growth, poor health  
and reduced reproductive performance in ruminants (Lengarite et al., 2012). This is corroborated by mineral results  
whereby, Ca and P levels of all forms of croton nut in this study were within the recommended critical maintenance level  
(1.2 - 2.6g/kg Ca) and (1.4g/kg P) respectively for ruminant animals (ARC, 1980). The K level in WN was above 8g/kg  
even though, the Mg level in all forms was below (2g/kg) recommended level for grazing animals, (Mirzaei, 2012). The  
level of Fe was above the recommended level (0.05g/kg) for grazing animals (ARC, 1980). Both DhN and DfS contained  
the recommended critical level of Zn (0.03g/kg) which is sufficient for cattle, sheep and goats (ARC, 1980).  
Removal of the husks and defatting effectively elevated CP content as reflected in DhN and DfS forms. The CP in all  
croton forms was above the recommended (80g/kg) required for maintenance in grazing ruminant animals (NRC, 2001).  
Moreover, DhN and DfS CP levels were within 140g/kg to 165g/kg recommended for growth and increased milk  
production in lactating animals (NRC, 2001). Defatting reduced the EE content considerably in DfS making it suitable for  
storage by reducing the amount of oils which when oxidised cause rancidity hence feed spoilage.  
Removal of the outer peel and husks (hard woody endocarp encasing the seeds) lowered the fibre levels  
considerably in DhN and DfS. Neutral detergent fibre level in these forms was between 450 g/kg to 650 g/kg. These  
forms may be classified as medium quality feed, a predominant characteristic of tropical feed stuffs (Singh and Oosting,  
1992). Feeds in this category can achieve the required gut health of ruminant animals by enhancing optimum feed  
intake, stimulating rumen function and increasing chewing of cud (Singh and Oosting, 1992). Moderate crude protein  
levels (80 90 g/kg) in WN and PN could play a fundamental role in mitigating lowered fibre digestibility that may be  
occasioned by the high NDF through availing of rumen ammonia nitrogen necessary for optimal functioning of the rumen  
ecosystem (Van Soest, 1994). There was no difference in NDICP among all forms of croton nut an indication that the  
degradability of insoluble-protein fraction was similar in all forms. NDICP represent the insoluble fraction of protein that  
remains after extraction with neutral detergent solution and is usually assumed to be insoluble (Mustafa et al., 2001).  
This fraction is a measure of nitrogen availability and constitutes a major portion of ruminal undegradable protein content  
High flavonoid content in all forms of croton nuts is an indication that croton nut could be included in ruminant feed  
rations to confer improved growth performance, health and improved rumen fermentation (Panche et al., 2016). A study  
by Kong et al. (2019) showed that flavonoid supplementation improved the average daily gain by alleviating stress during  
weaning of Holstein calves. Low level of tannins (<50 g/kg) similar to those recorded in this study could confer beneficial  
effects to ruminant animals such as reduction in ruminal protein degradation thus availing essential amino acids for  
absorption in the small intestines (Frutos et al., 2004). The level of aflatoxin observed in this study was within the  
minimum recommended level of 20ppb for complete and complementary feed materials used for feeding cattle, sheep  
and goats except for DhN (Kotinagu et al., 2015). The high level of aflatoxin in DhN could be attributed to high level of oil  
which provides conducive environment for growth of fungi resulting in production of aflatoxins (Filazi and Sireh, 2013).  
Therefore, proper handling and storage of DhN is crucial to prevent conditions that could encourage growth of fungi.  
In vitro gas production  
Amount of gas produced in in vitro gas digestibility method is an indicator of the rate and extent of feed digestion  
(Makkar, 2005). Gas production is affected by the composition, bioavailability of nutrients and presence of anti-nutritive  
factors in a feed. The higher levels of gas production observed in DfS compared to other forms of croton could be  
42  
Citation: Kabochi Njoroge E, Celina Wambui C and Bwire Wasike C (2021). Nutritional composition, in vitro gas production and in sacco degradability of processed  
Croton megalocarpus nuts for ruminant feeding. Online J. Anim. Feed Res., 11(2): 36-45. DOI: https://dx.doi.org/10.51227/ojafr.2021.7  
attributed to high levels of fermentable carbohydrates and protein which produce more gas when acted upon by rumen  
microbes (Makkar, 2005). Quality of roughage in a feed determines the nutritive value that the feed would confer when  
fed to an animal. The presence of high amount of fibre in a feed increases the rumen pool of indigestible fibre lignin  
which impedes the action of fibrolytic microbes that act on cellulose and hemicellulose (Venkateswarlu et al., 2013). This  
consequently reduces fermentable fibre as observed in PN.  
Observed reduced fermentation characteristics in DhN could be attributed to high levels of EE in this form. Although  
the type of fat was not differentiated in present study, presence of poly unsaturated fatty acids (PUFA) has been shown to  
reduce activity of fibre degrading microbes resulting to lower degradation and low gas production as observed in this  
study (Maia et al., 2010). It has been shown that excess oil of the long fatty acids in a feed (more than 3 - 5%) of the dry  
matter has a toxic effect on ruminal microorganisms especially bacteria which form the major fibrolytic colonies (Castillo-  
Gonzáleza et al., 2014). High predicted OMD and DMI in DfS implied better nutritive value in this form indicating that  
ruminant animals could consume higher amounts compared to the other forms (Negesse et al., 2016). The markedly high  
level of SCFA produced by DfS indicated that this form was better placed to supply the ruminant animals with the  
requisite energy to support production.  
In sacco degradability  
High dry matter degradability of rapidly degradable fraction (a) in DhN is an indication of high soluble nutrients  
which could be combined with low quality roughages to provide protein and energy needed by microbes. Slowly  
degradable fraction (b) of DM in all forms of croton nut was low compared to rapidly degradable fraction. Low fibre quality  
limit the ability of microbes in effectively degrading the feed by making it difficult for rumen microorganism to attach on  
the feed particles (Venkateswarlu et al., 2013). The dry matter rate constant of degradation (c) was comparable to various  
conventional feed resources such as coconut meal, peanut meal and whole cotton seeds (0.2-0.05 per hour)  
(Chumpawadee et al., 2005). This rate is important as it determines rumen fill and exerts direct effect on intake  
(Chumpawadee et al., 2005). At rumen outflow rate of kp=0.05, effective degradability (DM) of various forms of croton in  
this study were within the range (24.3 60.9%) observed for conventional protein sources which include soy bean meal,  
whole cotton seed, coconut meal and fish meal (Chumpawadee et al., 2005). This fraction represents the total amount of  
nutrients which can be captured by rumen microbes for their growth, production of VFAs and synthesis of microbial  
protein (Lanyasunya et al., 2006). The IV of all croton forms in this study were within the acceptable level of >33 as  
recommended by (Ørskov and Shand 1997). This level indicates sufficient nutrients that an animal needs to consume to  
meet its daily maintenance needs.  
The low level of rapidly soluble fraction of CP (a) observed in this study is within the recommended <40% for  
effective degraded protein (Lanyasunya et al., 2006). At this level, the (a) fraction does not overwhelm rumen microbes  
through production of excess nitrogen in form of ammonia, thus, maintaining an optimal protein-energy balance. Feeds  
with high slowly degradable fraction (b) avail required nitrogen in small amounts which are effectively utilized by rumen  
microbes. Effective degradability of crude protein provides an estimate of the total amount of protein captured by the  
rumen microbes for growth and synthesis of microbial protein (Lanyasunya et al., 2006). This fraction was high in DhN an  
indication that a considerable amount of protein in this form was degraded in the rumen. The remaining amount of  
protein regarded as rumen undegradable protein (RUP) represents the fraction of protein that is not degraded in the  
rumen and is termed as rumen by pass protein (Gao et al., 2015). Rumen by pass protein is available at the lower gut  
(small intestines) where combined with microbial protein contribute to protein requirements of the animal for  
maintenance and production. In this study WN was a good source of RUP and could be used to provide this form of protein  
in ruminant diets.  
CONCLUSION  
Processing through dehusking and defatting had the most significant impact on the nutritional composition of croton  
nuts. The two methods improved the nutritional profiles of protein, energy and mineral contents while reducing the fibre  
fractions compared to where peeling or no-processing was done. Degradability of dehusked and defatted forms of croton  
nuts was also high compared to the peeled and unprocessed whole nut forms. However, nutritional value of all forms of  
croton nuts was adequate and could be used in a total mixed ration (TMR) for maintenance purposes. In particular,  
dehusked and defatted forms have potential utilisation as protein supplements which could additionally supply energy  
and minerals for increased ruminant productivity on low quality basal diets. Microbial, enzymatic or chemical pre -  
treatment of the WN and PN forms prior to feeding could be explored to improve any observed lowered feed digestibility.  
Further studies to assess the effect of feeding croton on palatability, level of intake and production performance of  
ruminants are required.  
DECLARATIONS  
Corresponding author  
E-mail: wambuicc@gmail.com  
43  
Citation: Kabochi Njoroge E, Celina Wambui C and Bwire Wasike C (2021). Nutritional composition, in vitro gas production and in sacco degradability of processed  
Croton megalocarpus nuts for ruminant feeding. Online J. Anim. Feed Res., 11(2): 36-45. DOI: https://dx.doi.org/10.51227/ojafr.2021.7  
Authors’ contribution  
All authors contributed equally to this work.  
Conflict of interests  
The authors declare that there are no competing interests.  
Acknowledgements  
The authors thank Maseno University for provision of facilities to conduct the laboratory analyses, County  
Government of Laikipia for granting study leave to the first author and Kenya Climate Smart Agriculture Project (KCSAP)  
for funding this research.  
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Citation: Kabochi Njoroge E, Celina Wambui C and Bwire Wasike C (2021). Nutritional composition, in vitro gas production and in sacco degradability of processed  
Croton megalocarpus nuts for ruminant feeding. Online J. Anim. Feed Res., 11(2): 36-45. DOI: https://dx.doi.org/10.51227/ojafr.2021.7